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大连理工大学 精密与特种加工教育部重点实验室, 辽宁 大连 116024
[ "王紫光(1984-), 男, 辽宁大连人, 博士研究生, 2009年于辽宁石油化工大学获得学士学位, 2012年于大连交通大学获得硕士学位, 主要从事硬脆材料的精密与超精密加工研究.E-mail:wzg1107@mail.dlut.edu.cn" ]
康仁科(1962-), 男, 陕西西安人, 博士, 教授, 1984年、1987年、1999年在西北工业大学分别获得学士、硕士、博士学位, 主要研究方向为超精密加工与特种加工技术、难加工材料高效精密加工技术、半导体制造技术与设备, E-mail:kangrk@dlut.edu.cn KANG Ren-ke, E-mail:kangrk@dlut.edu.cn
收稿日期:2017-04-28,
录用日期:2017-5-19,
纸质出版日期:2017-10-25
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王紫光, 高尚, 朱祥龙, 等. 硅片低损伤磨削砂轮及其磨削性能[J]. 光学 精密工程, 2017,25(10):2689-2696.
Zi-guang WANG, Shang GAO, Xiang-long ZHU, et al. Grinding wheel for low-damage grinding of silicon wafers and its grinding performance[J]. Optics and precision engineering, 2017, 25(10): 2689-2696.
王紫光, 高尚, 朱祥龙, 等. 硅片低损伤磨削砂轮及其磨削性能[J]. 光学 精密工程, 2017,25(10):2689-2696. DOI: 10.3788/OPE.20172510.2689.
Zi-guang WANG, Shang GAO, Xiang-long ZHU, et al. Grinding wheel for low-damage grinding of silicon wafers and its grinding performance[J]. Optics and precision engineering, 2017, 25(10): 2689-2696. DOI: 10.3788/OPE.20172510.2689.
针对传统金刚石砂轮磨削硅片存在的表面/亚表面损伤问题,研制了一种用于硅片化学机械磨削加工的新型常温固化结合剂软磨料砂轮。根据化学机械磨削加工原理和单晶硅的材料特性,设计的软磨料砂轮以氧化铈为磨料,二氧化硅为添加剂,氯氧镁为结合剂。研究了软磨料砂轮的制备工艺,分析了软磨料砂轮的微观组织结构和成分。通过测量加工硅片的表面粗糙度、表面微观形貌和表面/亚表面损伤,进一步研究了软磨料砂轮的磨削性能。最后,与同粒度金刚石砂轮磨削和化学机械抛光(CMP)加工的硅片进行了对比分析。结果表明,采用软磨料砂轮磨削的硅片其表面粗糙度
R
a
<
1 nm,亚表面损伤仅为深度
<
30 nm的非晶层,远好于金刚石砂轮磨削硅片,接近于CMP的加工水平,实现了硅片的低损伤磨削加工。
A new Soft Abrasive Grinding Wheel (SAGW) was developed for Chemo-mechanical Grinding (CMG) of silicon wafers to overcome the surface/subsurface damage of the silicon wafer machined by traditional ultra-precision grinding. According to the principle of the CMG and the material characteristics of monocrystalline silicon
the SAGW took the cerium oxide (CeO
2
) as abrasive
silicon dioxide (SiO
2
)as additive
and the chlorine oxide magnesium as binding agent. The preparation process of the SAGW was investigated
and its microstructure and composition were analyzed. By measuring the surface roughness
surface microstructure and the surface/subsurface damage
the grinding performance of the SAGW was further explored. In the end
fabricated silicon wafer with the same particle size by the SAGW
Chemical Mechanical Polishing (CMP) and diamond grinding wheel was compared and analyzed. The results show that the surface roughness of the silicon wafer by the SAGW is less than 1 nm and its subsurface damage layer is about 30 nm in thickness
which is comparable to that produced by the CMG and much better than that of the diamond wheel. This study demonstrates that the developed SAGW achieves the low-damage grinding of silicon wafers.
ALVANOS T, GARANT J, ⅡJIMA Y, et al.. A novel methodology for wafer-specific feed-forward management of backside silicon removal by wafer grinding for optimized through silicon via reveal[C]. Proceedings of the 64th Electronic Components and Technology Conference (ECTC), IEEE, 2014: 452-458.
GIAGKA V, SAEIDI N, DEMOSTHENOUS A, et al.. Controlled silicon IC thinning on individual die level for active implant integration using a purely mechanical process[C]. Proceedings of the 64th Electronic Components and Technology Conference (ECTC), IEEE, 2014: 2213-2219.
DONG Z G, GAO S, HUANG H, et al.. Surface integrity and removal mechanism of chemical mechanical grinding of silicon wafers using a newly developed wheel[J]. International Journal of Advanced Manufacturing Technology, 2015, 83(5-8): 1231-1239.
张银霞, 郜伟, 康仁科, 等.单晶硅片磨削的表面相变[J].光学 精密工程, 2008, 16(8): 1440-1445.
ZHANG Y X, GAO W, KANG R K, et al.. Phase transformations of grinding monocrystalline silicon wafer surfaces[J]. Opt. Precision Eng., 2008, 16(8): 1440-1445. (in Chinese)
李敏, 袁巨龙, 吕冰海.剪切增稠抛光磨料液的制备及其抛光特性[J].光学 精密工程, 2015, 23(9): 2513-2521.
LI M, YUAN J L, LU B H. Preparation of shear thickening polishing abrasive slurries and their polishing properties[J]. Opt. Precision Eng., 2015, 23(9): 2513-2521. (in Chinese)
ZHONG Z W, TIAN Y B, NG J H, et al.. Chemical mechanical polishing (CMP) processes for manufacturing optical silicon substrates with shortened polishing time[J]. Materials and Manufacturing Processes, 2014, 29(1): 15-19.
许雪峰, 马冰迅, 黄亦申, 等.利用复合磨粒抛光液的硅片化学机械抛光[J].光学 精密工程, 2009, 17(7): 1587-1593.
XU X F, MA B X, HUANG Y SH, et al.. Chemical mechanical polishing for silicon wafer by composite abrasive slurry[J]. Opt. Precision Eng., 2009, 17(7): 1587-1593. (in Chinese)
ZHOU L B, KAWAI S, HONDA M, et al.. Research on chemo-mechanical-grinding (CMG) of Si wafer: 1st report: development of CMG wheel[J]. Journal of the Japan Society for Precision Engineering, 2002, 68(12): 1559-1563.
TIAN Y B, ZHOU L, SHIMIZU J, et al.. Elimination of surface scratch/texture on the surface of single crystal Si substrate in chemo-mechanical grinding (CMG) process[J]. Applied Surface Science, 2009, 255(7): 4205-4211.
HUANG H, WANG B L, WANG Y, et al.. Characteristics of silicon substrates fabricated using nanogrinding and chemo-mechanical-grinding[J]. Materials Science and Engineering: A, 2008, 479(1-2): 373-379.
GAO S, DONG Z G, KANG R K, et al.. Design and evaluation of soft abrasive grinding wheels for silicon wafers[J]. Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 2013, 227(4): 578-586.
BA H J, GUAN H. Influence of MgO/MgCl 2 molar ratio on phase stability of magnesium oxychloride cement[J]. Journal of Wuhan University of Technology-Materials Science Edition, 2009, 24(3): 476-481.
LI C D, YU H F. Influence of fly ash and silica fume on water-resistant property of magnesium oxychloride cement[J]. Journal of Wuhan University of Technology-Materials Science Edition, 2010, 25(4): 721-724.
YU J X, CHEN L, QIAN L M, et al.. Investigation of humidity-dependent nanotribology behaviors of Si(1 0 0)/SiO2 pair moving from stick to slip[J]. Applied Surface Science, 2013, 265: 192-200.
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