Test and analysis on nanohardness using an AFM-based system
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Test and analysis on nanohardness using an AFM-based system
Optics and Precision EngineeringVol. 15, Issue 5, Pages: 725-729(2007)
作者机构:
1. 佳木斯大学 机械工程学院,黑龙江 佳木斯,154007
2. 哈尔滨工业大学 精密工程研究所,黑龙江 哈尔滨 150001
作者简介:
基金信息:
DOI:
CLC:TH742.9
Received:25 October 2006,
Revised:02 February 2007,
Published Online:30 May 2007,
Published:30 May 2007
稿件说明:
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SHI Li-qiu, ZHANG Shun-guo, SUN Tao, et al. Test and analysis on nanohardness using an AFM-based system[J]. Optics and precision engineering, 2007, 15(5): 725-729.
DOI:
SHI Li-qiu, ZHANG Shun-guo, SUN Tao, et al. Test and analysis on nanohardness using an AFM-based system[J]. Optics and precision engineering, 2007, 15(5): 725-729.DOI:
Test and analysis on nanohardness using an AFM-based system
A system based on atomic force microscope(AFM) and a (Berkovich) diamond tip was developed for nanohardness and elastic modulus measurements. This system can directly gain the load-displacement curves that couldn't be obtained from indent software of AFM itself. The diamond tip was controlled by sending signal to achieve loading and unloading and gathering the real-time data. In this way the load-displacement curve and data could be acquired directly. Single point experiments were conducted on single-crystal copper and single-crystal aluminum thin films. TriboIndenter produced by Hysitron Inc was used to do the validated experiments. The results show that the system is suited for nanohardness measurement of the softer materials. By analysis on the effects of substrate material on nanohardness and elastic modulus
it can be known that the substrate has great influence on the mechanical characteristic of the film when the thickness of film is less than 5 to 10 times the peak depth. Nanohardness increases with a decrease in the indentation depth
which indicates a strong size effect
but there is no significant effect on the elastic modulus based the load-displacement curves.