SHEN Yong-hong, YAN Dong-mei, WANG Qi. Calcium fluoride crystal growth with multi-hole-crucible[J]. Optics and precision engineering, 2007, 15(10): 1474-1477.
SHEN Yong-hong, YAN Dong-mei, WANG Qi. Calcium fluoride crystal growth with multi-hole-crucible[J]. Optics and precision engineering, 2007, 15(10): 1474-1477.DOI:
Calcium fluoride crystal growth with multi-hole-crucible
By using a multi-hole-crucible and a furnace designed by ourselves
the CaF
2
crystals were grown by Bridgman-Stockbarger method under the vacuum condition. Under the growing condition of the vacuum below 3×10
-3
Pa
the axial gradient in growing zone about 1.8~2.5 ℃/mm
radial gradient below 0.5 ℃/mm
growing velocity of 3~4 mm/h and pre-annealing temperature descending velocity below 20 ℃/h
7 ingots of CaF
2
crystals with size of Φ57 mm×190 mm were grown in single process by melting
scavenging
homogenizing
controlling velocity and pre-annealing. The results show that the grown crystals with a wide transparent band have a good performance from 190 nm in ultra-violet to 9 000 nm in infra-red. The transmissivity is about 81% at 190 nm and 83% at 9 000 nm. The rate of mono-crystal is about 80%. The dislocation is about 30/mm
2
. The proposed equipment and technology are suited to batch production of CaF