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1.同济大学 物理科学与工程学院 精密光学工程技术研究所,先进微结构材料教育部;重点实验室,上海市数字光学前沿科学研究基地,上海市全光谱高性能光学薄膜器件与 应用专业技术服务平台,上海 200092
2.同济大学 中德工程学院,上海 200092
E-mail: wangzs@tongji.edu.cn
Received:15 July 2022,
Revised:22 August 2022,
Published:10 November 2022
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李文斌,李淑慧,潘刘洋等.薄膜反射镜纳秒极紫外辐照损伤[J].光学精密工程,2022,30(21):2698-2710.
LI Wenbin,LI Shuhui,PAN Liuyang,et al.Nanosecond extreme ultraviolet radiation damage on thin film mirrors[J].Optics and Precision Engineering,2022,30(21):2698-2710.
李文斌,李淑慧,潘刘洋等.薄膜反射镜纳秒极紫外辐照损伤[J].光学精密工程,2022,30(21):2698-2710. DOI: 10.37188/OPE.20223021.2698.
LI Wenbin,LI Shuhui,PAN Liuyang,et al.Nanosecond extreme ultraviolet radiation damage on thin film mirrors[J].Optics and Precision Engineering,2022,30(21):2698-2710. DOI: 10.37188/OPE.20223021.2698.
随着超短超强自由电子激光等光源的应用,极紫外、X射线波段薄膜反射镜的抗辐照性能备受关注。本文介绍了IPOE实验室搭建的纳秒极紫外辐照损伤装置,并对极紫外-X射线自由电子激光常用的B
4
C薄膜反射镜、Au和Ru金属单层膜反射镜、B
4
C/Ru双层膜反射镜以及极紫外光刻用Mo/Si多层膜反射镜开展了辐照损伤测试,获得了不同材料和结构的薄膜反射镜抗损伤性能,结合理论模拟揭示了热熔融、热应力和膜层间扩散反应等损伤机制的作用。
Owing to an increased application of novel light sources such as ultra-short and ultra-intense free electron lasers (FEL), damage resistance of extreme ultraviolet (EUV) and X-ray thin-film mirrors has attracted wide attention. This paper introduces a nanosecond EUV damage instrument manufactured by the Institute of Precision Optical Engineering (IPOE). EUV damage tests were conducted on boron carbide (B
4
C) reflective mirrors, gold (Au) and ruthenium (Ru) metal monolayer mirrors, B
4
C/Ru bilayer mirrors commonly used in EUV and X-ray free electron lasers, and molybdenum-silicon (Mo/Si) multilayer mirrors used in EUV lithography. Damage resistances for thin-film mirrors with different optical materials and structures were determined. Combined with theoretical simulations, damage mechanisms such as thermal melting, thermal stress, and interlayer diffusion-reaction were detected.
ULLRICH J , RUDENKO A , MOSHAMMER R . Free-electron lasers: new avenues in molecular physics and photochemistry [J]. Annual Review of Physical Chemistry , 2012 , 63 : 635 - 660 . doi: 10.1146/annurev-physchem-032511-143720 http://dx.doi.org/10.1146/annurev-physchem-032511-143720
赵振堂 , 王东 , 殷立新 , 等 . 上海软X射线自由电子激光装置 [J]. 中国激光 , 2019 , 46 ( 1 ): 33 - 42 . doi: 10.3788/cjl201946.0100004 http://dx.doi.org/10.3788/cjl201946.0100004
ZHAO ZH T , WANG D , YIN L X , et al . Shanghai soft X-ray free-electron laser facility [J]. Chinese Journal of Lasers , 2019 , 46 ( 1 ): 33 - 42 . (in Chinese) . doi: 10.3788/cjl201946.0100004 http://dx.doi.org/10.3788/cjl201946.0100004
BOSTEDT C , BOUTET S , FRITZ D M , et al . Linac Coherent Light Source: the first five years [J]. Reviews of Modern Physics , 2016 , 88 : 015007 . doi: 10.1103/revmodphys.88.015007 http://dx.doi.org/10.1103/revmodphys.88.015007
HUANG N S , DENG H X , LIU B , et al . Features and futures of X-ray free-electron lasers [J]. The Innovation , 2021 , 2 ( 2 ): 100097 . doi: 10.1016/j.xinn.2021.100097 http://dx.doi.org/10.1016/j.xinn.2021.100097
CHAPMAN H N , FROMME P , BARTY A , et al . Femtosecond X-ray protein nanocrystallography [J]. Nature , 2011 , 470 ( 7332 ): 73 - 77 .
泮丙营 , 叶茂 , 封东来 . X射线自由电子激光在物理学中的应用 [J]. 物理 , 2018 , 47 ( 7 ): 418 - 425 .
PAN B Y , YE M , FENG D L . The application of X-ray free electron lasers in physics [J]. Physics , 2018 , 47 ( 7 ): 418 - 425 . (in Chinese)
张文凯 , 孔庆宇 , 翁祖谦 . X射线自由电子激光在化学与能源材料科学中的应用 [J]. 物理 , 2018 , 47 ( 8 ): 504 - 514 . doi: 10.7693/wl20180803 http://dx.doi.org/10.7693/wl20180803
ZHANG W K , KONG Q Y , WENG Z Q . Applications of femtosecond X-ray techniques in chemistry and energy materials science [J]. Physics , 2018 , 47 ( 8 ): 504 - 514 . (in Chinese) . doi: 10.7693/wl20180803 http://dx.doi.org/10.7693/wl20180803
HAU-RIEGE S P , LONDON R A , BIONTA R M , et al . Damage threshold of inorganic solids under free-electron-laser irradiation at 32.5nm wavelength [J]. Applied Physics Letters , 2007 , 90 ( 17 ): 173128 . doi: 10.1063/1.2734366 http://dx.doi.org/10.1063/1.2734366
CHALUPSKÝ J , HÁJKOVÁ V , ALTAPOVA V , et al . Damage of amorphous carbon induced by soft X-ray femtosecond pulses above and below the critical angle [J]. Applied Physics Letters , 2009 , 95 ( 3 ): 031111 . doi: 10.1063/1.3184785 http://dx.doi.org/10.1063/1.3184785
GAUDIN J , PEYRUSSE O , CHALUPSKÝ J , et al . Amorphous to crystalline phase transition in carbon induced by intense femtosecond X-ray free-electron laser pulses [J]. Physical Review B , 2012 , 86 ( 2 ): 024103 . doi: 10.1103/physrevb.86.024103 http://dx.doi.org/10.1103/physrevb.86.024103
HAU-RIEGE S P , LONDON R A , BIONTA R M , et al . Wavelength dependence of the damage threshold of inorganic materials under extreme-ultraviolet free-electron-laser irradiation [J]. Applied Physics Letters , 2009 , 95 ( 11 ): 111104 . doi: 10.1063/1.3216845 http://dx.doi.org/10.1063/1.3216845
AQUILA A , SOBIERAJSKI R , OZKAN C , et al . Fluence thresholds for grazing incidence hard X-ray mirrors [J]. Applied Physics Letters , 2015 , 106 ( 24 ): 241905 . 46. doi: 10.1063/1.4922380 http://dx.doi.org/10.1063/1.4922380
HAU-RIEGE S P , LONDON R A , GRAF A , et al . Interaction of short X-ray pulses with low-Z X-ray optics materials at the LCLS free-electron laser [J]. Optics Express , 2010 , 18 ( 23 ): 23933 - 23938 . doi: 10.1364/oe.18.023933 http://dx.doi.org/10.1364/oe.18.023933
STOJANOVIC N , VON DER LINDE D , SOKOLOWSKI-TINTEN K , et al . Ablation of solids using a femtosecond extreme ultraviolet free electron laser [J]. Applied Physics Letters , 2006 , 89 ( 24 ): 241909 . doi: 10.1063/1.2405398 http://dx.doi.org/10.1063/1.2405398
MAKHOTKIN I A , MILOV I , CHALUPSKÝ J , et al . Damage accumulation in thin ruthenium films induced by repetitive exposure to femtosecond XUV pulses below the single-shot ablation threshold [J]. JOSA B , 2018 , 35 ( 11 ): 2799 - 2805 . doi: 10.1364/josab.35.002799 http://dx.doi.org/10.1364/josab.35.002799
KOYAMA T , YUMOTO H , SENBA Y , et al . Damage study of optical substrates using 1-μm-focusing beam of hard X-ray free-electron laser [J]. Journal of Physics: Conference Series , 2013 , 463 : 012043 . doi: 10.1088/1742-6596/463/1/012043 http://dx.doi.org/10.1088/1742-6596/463/1/012043
SVETINA C , MAHNE N , RAIMONDI L , et al . MagneDyn: the beamline for magneto dynamics studies at FERMI [J]. Journal of Synchrotron Radiation , 2016 , 23 ( 1 ): 98 - 105 . doi: 10.1107/s1600577515022080 http://dx.doi.org/10.1107/s1600577515022080
KOYAMA T , YUMOTO H , TONO K , et al . Damage threshold investigation using grazing incidence irradiation by hard X-ray free electron laser [C]. SPIE Optical Engineering+Applications. Proc SPIE 8848 , Advances in X-Ray/EUV Optics and Components VIII, San Diego, California, USA . 2013 , 8848 : 186 - 192 . doi: 10.1117/12.2025377 http://dx.doi.org/10.1117/12.2025377
MILOV I , MAKHOTKIN I A , SOBIERAJSKI R , et al . Mechanism of single-shot damage of Ru thin films irradiated by femtosecond extreme UV free-electron laser [J]. Optics Express , 2018 , 26 ( 15 ): 19665 - 19685 . doi: 10.1364/oe.26.019665 http://dx.doi.org/10.1364/oe.26.019665
FOLLATH R , KOYAMA T , LIPP V , et al . X-ray induced damage of B 4 C-coated bilayer materials under various irradiation conditions [J]. Scientific Reports , 2019 , 9 : 2029 . doi: 10.1038/s41598-019-38556-0 http://dx.doi.org/10.1038/s41598-019-38556-0
MILOV I , ZHAKHOVSKY V , ILNITSKY D , et al . Two-level ablation and damage morphology of Ru films under femtosecond extreme UV irradiation [J]. Applied Surface Science , 2020 , 528 : 146952 . doi: 10.1016/j.apsusc.2020.146952 http://dx.doi.org/10.1016/j.apsusc.2020.146952
FAENOV A , PIKUZ T , ISHINO M , et al . Soft X-ray laser ablation of metals and dielectrics [C]. SPIE Optics+Optoelectronics. Proc SPIE 10243, x-Ray Lasers and Coherent x-Ray Sources: Development and Applications, Prague, Czech Republic . 2017 , 10243 : 98 - 107 . doi: 10.1117/12.2264966 http://dx.doi.org/10.1117/12.2264966
ISHINO M , INOGAMOV N A , TAMOTSU S , et al . Study of damage structure formation on aluminum film targets by picosecond soft X-ray laser ablation around threshold region [J]. Applied Physics A , 2018 , 124 ( 9 ): 649 . doi: 10.1007/s00339-018-2072-9 http://dx.doi.org/10.1007/s00339-018-2072-9
MIKAMI K , ISHINO M , DINH T H , et al . Laser-induced damage thresholds and mechanism of silica glass induced by ultra-short soft X-ray laser pulse irradiation [J]. Optics Letters , 2020 , 45 ( 8 ): 2435 - 2438 . doi: 10.1364/ol.389288 http://dx.doi.org/10.1364/ol.389288
BARKUSKY F , PETH C , MANN K , et al . Formation and direct writing of color centers in LiF using a laser-induced extreme ultraviolet plasma in combination with a Schwarzschild objective [J]. Review of Scientific Instruments , 2005 , 76 ( 10 ): 105102 . doi: 10.1063/1.2072147 http://dx.doi.org/10.1063/1.2072147
BARKUSKY F , BAYER A , DÖRING S , et al . Damage threshold measurements on EUV optics using focused radiation from a table-top laser produced plasma source [J]. Optics Express , 2010 , 18 ( 5 ): 4346 - 4355 . doi: 10.1364/oe.18.004346 http://dx.doi.org/10.1364/oe.18.004346
ZHANG Z , LI W B , HUANG Q S , et al . A table-top EUV focusing optical system with high energy density using a modified Schwarzschild objective and a laser-plasma light source [J]. The Review of Scientific Instruments , 2018 , 89 ( 10 ): 103109 . doi: 10.1063/1.5044752 http://dx.doi.org/10.1063/1.5044752
LI W B , ZHANG Z , PAN L Y , et al . Table-top focused EUV optical system with high energy density and its application on EUV damage tests [C]. SPIE Optics+Optoelectronics. Proc SPIE 11035, Optics Damage and Materials Processing by EUV/X-Ray Radiation VII, Prague, Czech Republic . 2019 , 11035 : 1103505 . doi: 10.1117/12.2520143 http://dx.doi.org/10.1117/12.2520143
PAN L Y , ZHANG Z , LI W B , et al . Multiple pulses damage test on Mo/Si multilayer using table-top focused EUV optical system built at IPOE [C]. OSA High-brightness Sources and Light-driven Interactions Congress 2020 (EUVXRAY, HILAS, MICS). Washington D.C. : OSA , 2020 : ETh1A. 4 . doi: 10.1364/euvxray.2020.eth1a.4 http://dx.doi.org/10.1364/euvxray.2020.eth1a.4
LI W B , PAN L Y , WANG C L , et al . Multi-shot damage on Mo/Si multilayer induced by nanosecond EUV radiation [J]. AIP Advances , 2021 , 11 ( 1 ): 015201 . doi: 10.1063/5.0035490 http://dx.doi.org/10.1063/5.0035490
LI W B , WANG C L , PAN L Y , et al . Damage study on B 4 C films using a table-top nanosecond EUV damage instrument [C]. SPIE Optics+Optoelectronics. Proc SPIE 11776, EUV and x-Ray Optics, Sources, and Instrumentation , 2021 , 11776 : 109 - 116 . doi: 10.1117/12.2590040 http://dx.doi.org/10.1117/12.2590040
PAN L Y , LI S H , CAO J Y , et al . Ultrafast time-resolved pump-probe investigation of nanosecond extreme ultraviolet-light-induced damage dynamics on B 4 C/Ru nano-bilayer film [J]. Nano Letters , 2022 , 22 ( 13 ): 5260 - 5268 . doi: 10.1021/acs.nanolett.2c01171 http://dx.doi.org/10.1021/acs.nanolett.2c01171
BARKUSKY F , BAYER A , FLÖTER B , et al . Damage and degradation of optics and sensors under intense EUV radiation from a table-top laser produced plasma source [C]. Laser Damage Symposium XLI : Annual Symposium on Optical Materials for High Power Lasers. Proc SPIE 7504 , Laser-Induced Damage in Optical Materials: 2009, Boulder , Colorado , USA . 2009, 7504 : 521 - 530 .
CHALUPSKÝ J , JUHA L , KUBA J , et al . Characteristics of focused soft X-ray free-electron laser beam determined by ablation of organic molecular solids [J]. Optics Express , 2007 , 15 ( 10 ): 6036 - 6043 . doi: 10.1364/oe.15.006036 http://dx.doi.org/10.1364/oe.15.006036
CHALUPSKÝ J , BURIAN T , HÁJKOVÁ V , et al . Fluence scan: an unexplored property of a laser beam [J]. Optics Express , 2013 , 21 ( 22 ): 26363 - 26375 . doi: 10.1364/oe.21.026363 http://dx.doi.org/10.1364/oe.21.026363
WU J L , QI R Z , HUANG Q S , et al . Stress, roughness and reflectivity properties of sputter-deposited B 4 C coatings for X-ray mirrors [J]. Chinese Physics Letters , 2019 , 36 ( 12 ): 21 - 25 . doi: 10.1088/0256-307x/36/12/120701 http://dx.doi.org/10.1088/0256-307x/36/12/120701
付恩刚 , 庄大明 , 张弓 , 等 . 工作气压对磁控溅射ZAO薄膜性能的影响 [J]. 功能材料 , 2003 , 34 ( 5 ): 543 - 545 . doi: 10.3321/j.issn:1001-9731.2003.05.023 http://dx.doi.org/10.3321/j.issn:1001-9731.2003.05.023
FU E G , ZHUANG D M , ZHANG G , et al . Operation gas (argon) pressure dependence of the performances of ZAO thin films deposited by magnetron sputtering [J]. Journal of Functional Materials , 2003 , 34 ( 5 ): 543 - 545 . (in Chinese) . doi: 10.3321/j.issn:1001-9731.2003.05.023 http://dx.doi.org/10.3321/j.issn:1001-9731.2003.05.023
史新伟 , 周强 , 马群超 , 等 . 压强对直流磁控溅射TiN薄膜光学性能的影响 [J]. 郑州大学学报(理学版) , 2018 , 50 ( 4 ): 58 - 63 . doi: 10.13705/j.issn.1671-6841.2018060 http://dx.doi.org/10.13705/j.issn.1671-6841.2018060
SHI X W , ZHOU Q , MA Q CH , et al . Impact of pressure on the optical properties of TiN film prepared by DC magnetron sputtering [J]. Journal of Zhengzhou University (Natural Science Edition) , 2018 , 50 ( 4 ): 58 - 63 . (in Chinese) . doi: 10.13705/j.issn.1671-6841.2018060 http://dx.doi.org/10.13705/j.issn.1671-6841.2018060
冯秦旭 , 齐润泽 , 李文斌 , 等 . 涂硼中子探测器用B 4 C薄膜的应力和粘附力研究 [J]. 红外与激光工程 , 2019 ( S2 ): 74 - 80 .
FENG Q X , QI R Z , LI W B , et al . Stress and adhesion of B 4 C films for boron-coated neutron detectors [J]. Infrared and Laser Engineering , 2019 ( S2 ): 74 - 80 . (in Chinese)
LEE K M , HAN H J , CHOI S , et al . Effects of metal buffer layers on the hot filament chemical vapor deposition of nanostructured carbon films [J]. Journal of Vacuum Science & Technology B: Microelectronics and Nanometer Structures , 2003 , 21 ( 1 ): 623 . doi: 10.1116/1.1524136 http://dx.doi.org/10.1116/1.1524136
SWAB J J , MEREDITH C S , CASEM D T , et al . Static and dynamic compression strength of hot-pressed boron carbide using a dumbbell-shaped specimen [J]. Journal of Materials Science , 2017 , 52 ( 17 ): 10073 - 10084 . doi: 10.1007/s10853-017-1210-7 http://dx.doi.org/10.1007/s10853-017-1210-7
KOYAMA T , YUMOTO H , MIURA T , et al . Damage threshold of coating materials on X-ray mirror for X-ray free electron laser [J]. Review of Scientific Instruments , 2016 , 87 ( 5 ): 051801 . doi: 10.1063/1.4950723 http://dx.doi.org/10.1063/1.4950723
TAMURA K , OGASAKA Y , NAITOU M , et al . Measurements of reflectivity of X-ray mirror for Suzaku satellite [C]. SPIE Astronomical Telescopes+Instrumentation. Proc SPIE 6266, Space Telescopes and Instrumentation II : Ultraviolet to Gamma Ray, Orlando, Florida, USA . 2006 , 6266 : 991 - 998 . doi: 10.1117/12.671474 http://dx.doi.org/10.1117/12.671474
GÜDDE J , HOHLFELD J , MÜLLER J G , et al . Damage threshold dependence on electron-phonon coupling in Au and Ni films [J]. Applied Surface Science , 1998 , 127/ 128 / 129 : 40 - 45 .
SALAZAR A N . On thermal diffusivity [J]. European Journal of Physics , 2003 , 24 ( 4 ): 351 - 358 . doi: 10.1088/0143-0807/24/4/353 http://dx.doi.org/10.1088/0143-0807/24/4/353
FLECHSIG U , SPIELMANN S , THOMINET V , et al . Mirror systems for SwissFEL, from concept to commissioning with x-rays [C]. AIP Conference Proceedings. Taipei , China. Author(s) , 2019 , 2054 : 060001 . doi: 10.1063/1.5084632 http://dx.doi.org/10.1063/1.5084632
FOLLATH R , FLECHSIG U , MILNE C , et al . Optical design of the ARAMIS-beamlines at SwissFEL [J]. AIP Conference Proceedings , 2016 , 1741 ( 1 ): 020009 .
MILOV I , LIPP V , ILNITSKY D , et al . Similarity in ruthenium damage induced by photons with different energies: from visible light to hard X-rays [J]. Applied Surface Science , 2020 , 501 : 143973 . doi: 10.1016/j.apsusc.2019.143973 http://dx.doi.org/10.1016/j.apsusc.2019.143973
BAJT S , ALAMEDA J B , BARBEE T W J , et al . Improved reflectance and stability of Mo/Si multilayers [J]. Optical engineering , 2002 , 41 ( 8 ): 1797 - 1804 . doi: 10.1117/1.1489426 http://dx.doi.org/10.1117/1.1489426
KHORSAND A R , SOBIERAJSKI R , LOUIS E , et al . Single shot damage mechanism of Mo/Si multilayer optics under intense pulsed XUV-exposure [J]. Optics Express , 2010 , 18 ( 2 ): 700 - 712 . doi: 10.1364/oe.18.000700 http://dx.doi.org/10.1364/oe.18.000700
BAUDACH S , BONSE J , KRÜGER J , et al . Ultrashort pulse laser ablation of polycarbonate and polymethylmethacrylate [J]. Applied Surface Science , 2000 , 154/155 : 555 - 560 . doi: 10.1016/s0169-4332(99)00474-2 http://dx.doi.org/10.1016/s0169-4332(99)00474-2
KIM S H , SOHN I B , JEONG S . Ablation characteristics of aluminum oxide and nitride ceramics during femtosecond laser micromachining [J]. Applied Surface Science , 2009 , 255 ( 24 ): 9717 - 9720 . doi: 10.1016/j.apsusc.2009.04.058 http://dx.doi.org/10.1016/j.apsusc.2009.04.058
JEE Y , BECKER M F , WALSER R M . Damage Morphologies and Cumulative Behavior of Laser Damage on Single Crystal Metal Surfaces [M]. Laser Induced Damage in Optical Materials: 1986.100 Barr Harbor Drive , PO Box C700, West Conshohocken, PA 19428- 2959 : ASTM International, 2009 : 575-575 - 19 .
NEDELCU I , VAN DE KRUIJS R W E , YAKSHIN A E , et al . Thermally enhanced interdiffusion in Mo∕Si multilayers [J]. Journal of Applied Physics , 2008 , 103 ( 8 ): 083549 . doi: 10.1063/1.2907964 http://dx.doi.org/10.1063/1.2907964
TAKENAKA H , KAWAMURA T , ISHII Y , et al . Heat resistance of Mo/Si, MoSi 2 /Si, and Mo 5 Si3/Si multilayer soft X-ray mirrors [J]. Journal of Applied Physics , 1995 , 78 ( 9 ): 5227 - 5230 . doi: 10.1063/1.359698 http://dx.doi.org/10.1063/1.359698
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