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摘要:目的:为解决采用AFM系统进行纳米机械性能测试中存在的不能够直接获得载荷——压深曲线以及不能够随意改变加载、保载、卸载时间等问题,对AFM系统进行改造。方法:开发了一套基于单片机的信号输入输出模块。将该模块与AFM控制系统相联,形成新的纳米机械性能测试系统。结果:该系统可以实现动态改变垂直载荷,并依据相应算法,可以实现载荷——压深曲线的实时获得。通过单片机设置模拟信号的输出速率可以实现加载、保载和卸载速率的改变。并结合二维微动精密工作台,可以实现较大范围内点阵的压痕测试。结论:通过在聚碳酸酯、聚二甲基硅氧烷等材料表面进行试验测试表明:该系统可以进行高速高精度的测量样品的纳米机械性能参数,包括对样品进行纳米压痕测试和对样品的纯弹性变形过程进行检测如聚二甲基硅氧烷或者各种微梁等微小构件。
Abstract: Objective: To resolve problems of AFM in the applications of measurement of nanomechanical properties of samples such as: the force-depth curve can not be obtained directly and the loading time
keeping time at the peak load and the unload time can not be varied arbitrarily
and so on
AFM system is modified. Mehotd: A Single Chip Micyoco (SCM)-based input/output module is developed in the present study. This module is connected to the control system of AFM
forming a novel AFM-based nanomechanical property measurement system. Result:The normal load can be changed continuously. According to the corresponding arithmetic
the in-situ force-depth curve can be achieved. The out rate of the D/A output port can be varied by the SCM controller
which can change the rate of loading
unloading and keeping period. Integrated with a two-dimensional precision stage
the array indentation tests can be carried out with a larger scale. Conclusion: Nanoindentation tests on polycarbonate and Polydimethylsiloxane show that based on this system
the nanomechanical properties parameters of samples can be achieved with high accuracy and high speed. Samples like PDMS
micro beam and so on can also be investigated under the pure elastic deformation.
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