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1.哈尔滨理工大学 测控技术与通信工程学院, 黑龙江 哈尔滨 150080
2.苏州大学 机电工程学院, 江苏 苏州 215301
[ "王鑫(1983-), 女, 黑龙江人, 副教授, 博士研究生, 2005年、2008年于哈尔滨理工大学分别获得学士、硕士学位, 主要研究方向为MEMS传感器及微系统。E-mail:wangxin6711545@163.com" ]
施云波(1966-), 男, 吉林人, 教授, 博士生导师, 1987年于天津大学获得学士学位, 2002年于福州大学获得硕士学位, 2008年于哈尔滨理工大学获得博士学位, 现为哈尔滨理工大学测控技术与通信工程学院系主任, 主要研究方向为MEMS传感器及微系统, 测试和系统集成技术。E-mail:shiyunbo@hrbust.edu.cn SHI Yun-bo, E-mail:shiyunbo@hrbust.edu.cn
收稿日期:2020-04-30,
修回日期:2020-06-01,
录用日期:2020-6-1,
纸质出版日期:2020-10-25
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王鑫, 施云波. 微型多参数水质传感器芯片的设计及应用[J]. 光学 精密工程, 2020,28(10):2215-2226.
Xin WANG, Yun-bo SHI. Design and application of miniature multi-parameter water quality sensor chip[J]. Optics and precision engineering, 2020, 28(10): 2215-2226.
王鑫, 施云波. 微型多参数水质传感器芯片的设计及应用[J]. 光学 精密工程, 2020,28(10):2215-2226. DOI: 10.37188/OPE.20202810.2215.
Xin WANG, Yun-bo SHI. Design and application of miniature multi-parameter water quality sensor chip[J]. Optics and precision engineering, 2020, 28(10): 2215-2226. DOI: 10.37188/OPE.20202810.2215.
针对目前水质参数传感器测量功能单一,且受环境温度影响大等问题,提出了一种具有温度补偿功能的多参数水质传感器芯片。该传感器芯片是使用微机电系统(MEMS)技术制造的,芯片表面集成了pH传感器、DO传感器、氨氮传感器和温度传感器。为实现温度补偿,芯片还设计了一种夹心板式蛇形Pt电阻加热器。同时设计了与芯片相适应的微流控测试腔,以实现水样测量。采用有限元稳态热分析对4种加热器热传递过程进行分析,得到合理的芯片结构布局,通过MEMS工艺制作出传感器芯片。采用自制的恒电位仪测试电路,对传感器芯片性能进行了测试。实验结果表明,pH传感器具有0.288 mA/pH的高灵敏度;溶解氧(DO)传感器的灵敏度为2.22
μ
A/(mg·L
-1
);氨氮传感器的灵敏度为0.113 9 mA/(mg·L
-1
);温度传感器的灵敏度为0.949 Ω/℃;加热器的功率和温度变化灵敏度为0.312 6℃/mW。与单个水质参数传感器相比,该传感器芯片体积小、坚固耐用,能够同时检测水样的多种参数,且温度补偿效果较好。
Water-quality sensors feature a single measurement function and are greatly affected by ambient temperature. This paper proposes a multi-parameter water-quality sensor chip with temperature compensation. The sensor chip was manufactured using the micro-electro-mechanical system (MEMS) technology. The chip surface contained integrated pH
dissolved oxygen (DO)
ammonia-nitrogen
and temperature sensors. To achieve temperature compensation
the chip was also designed with a sandwich-plate snake Pt resistance heater. At the same time
a microfluidic test chamber that was matched with the chip was designed to realize water-sample measurement. Finite-element steady-state thermal analysis was used to analyze the heat-transfer process of four heaters
and a reasonable chip-structure layout was established. Thereafter
the sensor chip was fabricated using the MEMS technology. The performance of the sensor chip was investigated using a laboratory-developed potentiostat test circuit. Experimental results show that the pH sensor has a high sensitivity of 0.288 mA/pH.The sensitivity of the temperature sensor is 0.949 Ω/℃ and that of the ammonia-nitrogen sensor was 0.113 9 mA/(mg·L
-1
). The sensitivity of the DO sensor is 2.22
μ
A/(mg·L
-1
) and that of the temperature sensor
which changes with respect to the heater power
is 0.312 6 ℃/mW. Compared with a single water-quality parameter sensor
the as-prepared sensor chip could simultaneously detect multiple parameters of a water sample and exhibited a good temperature-compensation effect. Moreover
the sensor chip was small in size
robust
and highly accurate.
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