用光纤耦合法实现颗粒测量

隋国荣; 程利; 陈抱雪

doi:10.3788/OPE.20111912.2844

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用光纤耦合法实现颗粒测量

现代应用光学 | 更新时间：2020-08-12

- 用光纤耦合法实现颗粒测量
- Measurement of particles by optical fiber coupling
- 光学精密工程 2011年19卷第12期页码：2844-2853
- 作者机构：
  
  上海理工大学光电信息与计算机工程学院上海,200093
- 作者简介：
- 基金信息：
  
  国家自然科学基金资助项目(No.61077042/F050211)();上海市重点学科建设资助项目(No.S30502)();上海理工大学光电学院教师创新能力建设项目(
- DOI：10.3788/OPE.20111912.2844
  中图分类号： O436.3;TN253
- 收稿日期：2011-04-19，
  
  修回日期：2011-05-26，
  
  网络出版日期：2011-12-25，
  
  纸质出版日期：2011-12-25
- 稿件说明：
移动端阅览
隋国荣, 程利, 陈抱雪. 用光纤耦合法实现颗粒测量[J]. 光学精密工程, 2011,19(12): 2844-2853

SUI Guo-rong, CHENG Li, CHEN Bao-xue. Measurement of particles by optical fiber coupling[J]. Editorial Office of Optics and Precision Engineering, 2011,19(12): 2844-2853
隋国荣, 程利, 陈抱雪. 用光纤耦合法实现颗粒测量[J]. 光学精密工程, 2011,19(12): 2844-2853 DOI： 10.3788/OPE.20111912.2844.

SUI Guo-rong, CHENG Li, CHEN Bao-xue. Measurement of particles by optical fiber coupling[J]. Editorial Office of Optics and Precision Engineering, 2011,19(12): 2844-2853 DOI： 10.3788/OPE.20111912.2844.

摘要

根据全光散射法测量粒径存在样品池壁散射及折射率改变等问题

提出了利用光纤耦合结构

并引入洛伦兹经典色散公式和多波长处理方法来实现颗粒测试。首先

介绍了全光散射法进行颗粒测试的理论

并研究现有的样品池和测量手段存在的问题。然后

引入洛伦兹色散公式来处理折射率的变化;同时结合多波长处理法

获得颗粒的平均粒径和粒径分布公式

建立目标函数并利用遗传算法进行参数反演;通过光纤端面的耦合结构构造样品池

利用光谱仪对夹在光纤端面间的待测液进行多波长扫描。最后

试制了实际测试系统

通过计算机内部算法

完成颗粒测试。仿真和实验结果表明

该方法可以在折射率未知的情况下较准确地反演出颗粒的平均粒径及其粒径分布;对测量光谱加入2%的随机噪声后

其平均粒径及折射率的反演误差低于1%

粒径分布的反演误差低于5%

可以满足国标对均值误差和重复性误差的要求。

Abstract

By using an optical fiber coupling structure

a new particle measuring method through introducing Lorentz classic dispersion formula and multi-wavelength processing was proposed to amend the scattering influence of a sample cell wall and the change of the refractive index. Firstly

the theory of total light scattering for the particle measurement was introduced

and the problems existied in the sample cell and measurement method were studied. Then

the Lorentz dispersion formula was introduced to process the refractive index changes caused by dispersion and the multi-wave length processing was taken to obtain the average particle size and particle size distribution. By establishing an object function

a method based on the genetic algorithm was proposed to implement the inversion of particle refractive index. A new sample cell was designed and manufactured with the end face coupling of optical fiber

and the particle sample dripping placed the end face between two optical fibers was scanned by a spectrometer in multi-wavelengths.Finally

through the algorithm of the computer

the average particle size and particle size distribution were measured. The simulation and experiment result indicates that the average particle size and particle size distribution can be well determined by this method in the case of unknown refractive index.Furthermore

this method has advantages of reliability and stability. When a 2% random noise was put in the transmission extinction measurement values at two wavelengths

the inversion errors of average particle size and refraction index are less than 1% and that of the particle size distribution is less than 5%. It can meet the needs of national standard for mean errors and repeatability errors.

关键词

Keywords

references

MARIE J D, IAN A C, RICHARD J M. Determination of particle size distribution by laser diffraction of doped-CeO2 powder suspensions: effect of suspension stability and sonication[J]. Part.Syst.Charact., 2006, 22(5):310-319.[2] WEDD M W. Determination of particle size distributions using laser diffraction[J]. Educ.Resour.Part.Technol., 2003, 32:1-4.[3] 吴立敏, 盛克平, 王虎. 光子相关光谱法对颗粒平均粒径测量结果的不确定度评定[J]. 理化检验-物理分册, 2005, 41(5):245-249. WU L M, SHENG K P, WANG H. Evaluation of uncertainty for particle size analysis by photon correlation spectroscopy[J]. Ptca(Part:a Phys. Test.), 2005, 41(5):245-249. (in Chinese)[4] 王燕民, 陈琪星, 潘志东. 激光粒度测量的综合反演及参数选择[J]. 光学精密工程, 2009, 17(9):2120-2127. WANG Y M, CHEN Q X, PAN ZH D. Hybrid inversion algorithm for laser scattering particle size analyzer and its parameter selection[J]. Opt.Precision Eng.,2009,17(9):2120-2127. (in Chinese)[5] 徐峰, 蔡小舒, 苏明旭,等. 光谱消光法测量高压湿蒸汽的研究[J]. 动力工程, 2009, 29(3):254-261. XU F, CAI X SH, SU M X, et al. Research on the measurement of high pressure wet steam by spectral light extinction method[J]. Journal of Power Engineering, 2009, 29(3):254-261. (in Chinese)[6] 杨晖, 郑刚, 王雅静. 用动态光散射现代谱估计法测量纳米颗粒[J]. 光学精密工程, 2010, 18(9):1996-2001. YANG H, ZHENG G, WANG Y J. Measurement of nano-particles by dynamic light scattering based on spectral estimation[J]. Opt.Precision Eng., 2010, 18(9):1996-2001. (in Chinese)[7] 何新, 贾红辉, 常胜利, 等. 多次散射情况下非视线光传输的模拟[J]. 光学精密工程, 2009, 17(2):246-250. HE X, JIA H H, CHANG SH L, et al. Simulation of non-line-of-sight light propagation for multiple-scattering instance[J]. Opt.Precision Eng., 2009, 17(2):246-250. (in Chinese)[8] 唐红, 郑文斌, 李宪霞. 主成分分析在光全散射特征波长选择中的应用[J]. 光学精密工程, 2010, 18(8):1691-1698. TANG H, ZHENG W B, LI X X. Application of principal component analysis to selection of characteristic wavelengths with total light scattering[J]. Opt.Precision Eng., 2010, 18(9):1691-1698. (in Chinese)[9] 苏明旭, 任宽芳, Grehan G, 等. 光复散射对消光法粒径测量的影响:复散射模型与数值模拟[J]. 光学学报, 2004, 24(5):696-699. SU M X,REN K F,GREHAN G,et al. The affect of light multiple scattering on particle sizing by using light extinction method[J]. Acta Optica Sinica, 2004, 24(5):696-699. (in Chinese)[10] 徐峰, 蔡小舒, 苏明旭, 等. 独立模式算法求解颗粒粒径分布的研究[J]. 中国激光, 2004, 31(2):223-228. XU F, CAI X SH, SU M X, et al. Study of independent model algorithm for determination of particle size distribution[J]. Chinese Journal of Laser, 2004,31(2):223-228. (in Chinese)[11] 徐峰, 蔡小舒, 任宽芳, 等. 遗传算法在多光谱消光法测量粒径中的应用[J]. 中国颗粒学报, 2004, 2(6):235-240. XU F, CAI X SH, REN K F, et al. Application of genetic algorithm in particle size analysis by multispectral extinction measurements[J]. China Particuology, 2004,2(6):235-240. (in Chinese)[12] 王少清, 董学仁, 孙平. 矩形样品池对激光粒度测量的影响及其修正[J]. 光学技术, 2002, 28(3):259-260. WANG SH Q, DONG X R, SUN P. Affection of square sample sell on laser particle sizing and its correction[J]. Optical Technology, 2002, 28(3):259-260. (in Chinese)[13] 杨晖, 郑刚, 李孟超, 等. 后向动态光散射测量中样品池的影响及校正[J]. 光散射学报, 2008, 20(4):306-309. YANG H, ZHENG G, LI M CH, et al. Affection of sample cell in dynamic light back scattering measurement and its correction[J]. The Journal of Light Scattering, 2008, 20(4):306-309. (in Chinese)[14] 王乃宁. 颗粒粒径的光学测量技术及应用[M]. 北京:原子能出版社, 2000. WANG N N. Optic Measurement Technology of Particle Size and Its Application[M]. Beijing:Atomic Energy Press, 2000.(in Chinese)[15] 叶玉堂, 饶建珍, 肖峻. 光学教程[M]. 北京:清华大学出版社,2005. YE Y T, RAO J ZH, XIAO J. Optics Course[M]. Beijing: Tsinghua University Press, 2005.(in Chinese)[16] 张虎, 戴景民, 唐红, 等. 改进的遗传算法在粒径测量中的应用[J]. 光电工程, 2008, 35(9):50-54. ZHANG H, DAI J M, TANG H, et al. Application of improved genetic algorithm in the particle sizing technique[J]. Opto-Electronic Engineering, 2008, 35(9):50-54. (in Chinese)[17] 孙晓刚, 唐红, 原桂彬. 颗粒系的可见消光光谱分析及最佳波长的选择[J]. 光谱学与光谱分析, 2008, 28(9):1968-1973. SUN X G, TANG H, YUAN G B. Analysis of visible extinction spectrum of particle system and selection of optimal wavelength[J]. Spectroscopy and Spectral Analysis, 2008, 28(9):1968-1973. (in Chinese)[18] 刘铁英, 郑刚, 虞先煌, 等. 三波长消光法测定微粒的粒径及其分布[J]. 仪器仪表学报, 2000, 21(2):208-210. LIU T Y, ZHENG G, YU X H, et al. A method to determine size distribution of small particles using three wavelengths extinction[J]. Chinese Journal of Scientific Instrument, 2000, 21(2):208-210. (in Chinese)[19] 孙晓刚, 唐红, 原桂彬. 非独立模式算法下粒径分布反演及分类的研究[J]. 光谱学与光谱分析, 2008,28(5):1111-1114. SUN X G, TANG H, YUAN G B. Study of inversion and classification of particle size distribution under dependent model algorithm[J]. Spectroscopy and Spectral Analysis, 2008, 28(5):1111-1114. (in Chinese)[20] MALITSON I H. Interspecimen comparison of the refractive index of fused silica[J]. Opt. Soc. Am., 1965, 55(9):1205-1209.[21] 郑刚, 卫敬明, 王乃宁. 用多波长消光法测量大颗粒的尺寸分布[J]. 光学学报, 1993, 13(2):165-169. ZHENG G, WEI J M, WANG N N. Determination of size distribution of large particle using multi-wavelength light extinction[J]. Acta Optica Sinica, 1993, 13(2):165-169. (in Chinese)

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