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中国科学院 长春光学精密机械与物理研究所,吉林 长春,中国,130033
[ "董斌超(1986-),男,陕西咸阳人,硕士,研究实习员,2009年于湖南大学获得学士学位,2012年于西安交通大学获得硕士学位,主要从事轻型碳化硅反射镜制备技术的研究。E-mail:dbczyg@163.com" ]
[ "张舸(1980-),男,重庆荣昌人,副研究员,2003年于长春理工大学获得学士学位,2008年于中国科学院长春光学精密机械与物理研究所获得博士学位,主要从事轻型碳化硅反射镜制备技术的研究。E-mail:zhanggeciomp@126.com" ]
收稿日期:2015-04-02,
修回日期:2015-05-19,
纸质出版日期:2015-08-25
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董斌超, 张舸,. 超轻量化SiC反射镜的制备及性能[J]. 光学精密工程, 2015,23(8): 2185-2191
DONG Bin-chao, ZHANG Ge,. Fabrication and properties of ultra-lightweight SiC mirror[J]. Editorial Office of Optics and Precision Engineering, 2015,23(8): 2185-2191
董斌超, 张舸,. 超轻量化SiC反射镜的制备及性能[J]. 光学精密工程, 2015,23(8): 2185-2191 DOI: 10.3788/OPE.20152308.2185.
DONG Bin-chao, ZHANG Ge,. Fabrication and properties of ultra-lightweight SiC mirror[J]. Editorial Office of Optics and Precision Engineering, 2015,23(8): 2185-2191 DOI: 10.3788/OPE.20152308.2185.
采用真空辅助凝胶注模和反应烧结法制备了面密度分别为9.35和11.7 kg/m
2
直径分别为200和500 mm的两块超轻量化SiC反射镜
检测了反射镜的主要性能。结果显示:由于在真空环境下浇注
坯体没有宏观缺陷。材料中细小SiC颗粒的存在使材料具有相对较高的抗弯强度(335 MPa)和断裂韧性(4.5MPa· m
1/2
)。此外
反射镜材料金相组织中未出现明显的SiC颗粒定向排列
具有较好的各向同性度:不同方向热膨胀系数差异小于3%
模量差异为1.3%。镜坯经过光学加工后面形误差(RMS值)为0.043λ(λ=632.8 nm)
表面粗糙度(
R
a
值)优于5 nm。实验表明
真空辅助凝胶注模成型结合反应烧结工艺制备的超轻量化SiC反射镜各方面性能良好
适用于制备空间相机用反射镜。
Vacuum pressure assisted gel-casting and reaction sintering were applied to fabrication of
Φ
200 and
Φ
500mm ultra-lightweight SiC mirrors with the area densities of 9.17 kg/m
2
and 10.8 kg/m
2
respectively. The main properties of the SiC mirrors were tested. The results show that the green bodies of the SiC mirrors have no macroscopic defects due to its pouring in a vacuum environment. The mirror materials have high flexural strength (335 MPa) and fracture toughness (4.5 MPa· m
1/2
) because of the fine SiC particles. The metallographic structures of the mirror materials do not show the directional alignment of SiC particles
which means the mirror materials possess a high isotropy ratio
in which the relative deviation of Coefficient of Thermal Expansion(CTE) is less than 3%
and the relative deviation of modulus reaches 1.3%. After polishing
the surface profile accuracy (RMS) of the mirror is 0.043λ (λ=632.8 nm)
and the toughness is better than 5 nm. These results demonstrate that the ultra-lightweight SiC mirrors fabricated by vacuum-assisted gel-casting and reaction sintering have excellent performance
and are suitable for fabrication of the mirrors of space cameras.
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