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纳米Fe-Al/Cr3C2复合涂层的抗电化学腐蚀性能
Electrochemical corrosion resistance property of nano Fe-Al/Cr3C2 composite coating
- 光学 精密工程 2019年27卷第9期 页码：1950-1959
- 作者机构：
1.内蒙古电力科学研究院, 内蒙古 呼和浩特 010020
2.内蒙古工业大学 材料科学与工程学院, 内蒙古 呼和浩特 010020
3.内蒙古自治区薄膜与涂层重点实验室, 内蒙古 呼和浩特 010051
4.内蒙古能源发电金山热电有限公司, 内蒙古 呼和浩特 010106
- 作者简介：
[ "刘晓明(1978-)，男，内蒙古呼和浩特人，博士，高级工程师，2004年于内蒙古工业大学获得硕士学位，2012年于内蒙古工业大学获得博士学位，现为内蒙古电力科学研究院设备材料技术中心副主任，主要从事电力系统微/纳米涂层材料研发、涂层制备及应用的研究。E-mail:31535029@qq.com" ]
[ "马文(1973-)，男，内蒙古巴彦淖尔人，博士，教授，博士生导师，2002年于北京科技大学获得硕士学位，2006年于北京航空航天大学获得博士学位，主要从事热障涂层、耐磨涂层、功能陶瓷的制备与应用。E-mail：wma@imut.edu.cn" ]
- 基金信息：内蒙古电力(集团)有限责任公司2019年第1批科技项目(201901097)
DOI：10.3788/OPE.20192709.1950
中图分类号： TB853.29收稿日期：2019-05-21，
录用日期：2019-7-15，
纸质出版日期：2019-09-15
- 稿件说明：
移动端阅览
刘晓明, 马文, 闫侯霞, 等. 纳米Fe-Al/Cr3C2复合涂层的抗电化学腐蚀性能[J]. 光学 精密工程, 2019,27(9):1950-1959.
Xiao-ming LIU, Wen MA, Hou-xia YAN, et al. Electrochemical corrosion resistance property of nano Fe-Al/Cr3C2 composite coating[J]. Optics and precision engineering, 2019, 27(9): 1950-1959.
刘晓明, 马文, 闫侯霞, 等. 纳米Fe-Al/Cr3C2复合涂层的抗电化学腐蚀性能[J]. 光学 精密工程, 2019,27(9):1950-1959. DOI： 10.3788/OPE.20192709.1950.
Xiao-ming LIU, Wen MA, Hou-xia YAN, et al. Electrochemical corrosion resistance property of nano Fe-Al/Cr3C2 composite coating[J]. Optics and precision engineering, 2019, 27(9): 1950-1959. DOI： 10.3788/OPE.20192709.1950.
摘要
研究纳米Fe-Al/Cr
3
C
2
复合涂层的抗电化学腐蚀性能，确定纳米Fe-Al/Cr
3
C
2
团聚颗粒加入量的最佳值。采用三电极系统，对微米Fe-Al/Cr
3
C复合涂层、纳米Fe-Al/Cr
3
C
2
和分别添加了5%，10%，15%纳米Fe-Al/Cr
3
C
2
团聚颗粒的系列复合涂层抗电化学腐蚀性能进行测试；利用Zview软件拟合交流阻抗谱，从定性到定量拟合对纳米Fe-Al/Cr
3
C
2
系列复合涂层的电化学腐蚀行为进行分析；利用扫描电子显微镜观察腐蚀后涂层表面形貌。添加了5%纳米Fe-Al/Cr
3
C
2
团聚颗粒的复合涂层自腐蚀电位为-0.775 V，自腐蚀电流为0.280 mA/cm
2
，与其它涂层相比抗电化学腐蚀性能最优；此处添加的5%纳米级Fe-Al/Cr
3
C
2
团聚颗粒的复合涂层的特征主要以均匀腐蚀性为主，而其它Fe-Al/Cr
3
C
2
复合涂层都表现为一定的局部腐蚀特性。Fe-Al/Cr
3
C
2
复合涂层本身的抗电化学腐蚀特性会受到Fe-Al/Cr
3
C
2
团聚颗粒的影响而存在改善的价值。加入量低于最佳值时，涂层因表面质量没有得到改善而抗电化学腐蚀性能较低；加入量高于最佳值时，涂层因表面高活性而导致抗电化学腐蚀性能较低。
Abstract
The electrochemical corrosion resistance properties of nano Fe-Al/Cr
3
C
2
composite coating were tested. The ideal amount of nano Fe-Al/Cr
3
C
2
reunion-granulation particle to be added was determined. Using three-electrode system
the electrochemical corrosion resistance properties of five kinds Fe-Al/Cr
3
C
2
composite coatings were tested. These were micro Fe-Al/Cr
3
C
2
composite coating
nano Fe-Al/Cr
3
C
2
composite coating
and composite coating with additional 5%
10%
and 15% nano Fe-Al/Cr
3
C
2
reunion-granulation particles
respectively. Zview software was used to fit the AC impedance spectrum in order to analyze the electrochemical corrosion resistance action of coatings. SEM was used to analyze the corrosion surface of coatings. The results indicate that the best electrochemical corrosion resistance property of composite coatings was obtained by adding 5% nano Fe-Al/Cr
3
C
2
reunion-granulation particles. Compared with other coatings
the coating with added 5% nano Fe-Al/Cr
3
C
2
reunion-granulation particles has maximum self-corrosion potential of -0.775 V and minimum self-corrosion current of 0.280 mA/cm
2
. When the content of nano granulated particles is lower than the optimum value
the electrochemical corrosion resistance properties of coatings are because the content of nano granulated particles is too low to improve density and reduce pore size. When the content of nano granulated particles is higher than the optimum value
the electrochemical corrosion resistance property of coatings are nano granulated particles makes surface of coatings showing high chemical energy.
关键词
Keywords
references
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